SINTESIS SENYAWA AURIVILLIUS LAPIS EMPAT PbBi4-xNdxTi4O15 DENGAN METODE LELEHAN GARAM
Abstract: Aurivillius phase
is a metal
oxide compound with
general formulae [Bi2O2]2+[An-1BnO3n+1]2-. Four layers
Aurivillius phase, PbBi4-xNdxTi4O15 with x = 0.5 and x = 1 had been synthesized
by using molten salt method where salt mixture was Na2SO4/K2SO4 (1:1) as the flux. The samples were heated
at 750oC for
10 hours, 850oC
for 5 hours,
and 950oC for
5 hours. Polycrystallines were characterized
by X-Ray Diffractometer (XRD).
All XRD data
were refined by
RIETICA program with Le
Bail method. The
results show that
all samples have
performed four layers Aurivillius phase
however another phase
was also observed
for both samples
predicted as Bi7.7Ti0.3O12.16.
The volume cell of four layers Aurivillius compound increases with increasing
the value of x.
Penulis: Habil Lutfi, Syukri
Arief, Zulhadjri
Kode Jurnal: jpkimiadd150279
