PENETAPAN KADAR KUMARIN DARI KULIT MANIS (Cinnamomum burmanii Bl.) DENGAN METODA KROMATOGRAFI GAS
ABSTRACT: The qualitative and quantitative analysis
of coumarin in cinnamon (Cinnamomum burmanii Bl.) which are qualified in to AA, KA and KB has been
done by gas chromatography and gas chromatography-mass spectrometry.
Extraction of quality
KB coumarin was
carried out by soxchletation in
hexane, dichloromethane and
methanol. Meanwhile, quality
AA and KA coumarins
are soxchletated in
methanol. The qualitative analysis using gas
chromatographymass
spectrometry with column
BP-5 showed that
hexane, dichloromethane and
methanol extracts of qualified KB coumarin, as well as methanol extracts
of qualified AA and KB only contain coumarin
compounds, no other
coumarin groups were
found. From coumarin quantitative analysis
by gas chromatography using
BP-624 column and
FID detector of methanol
extracts obtained 1855.51
ppm (0.186%), 1915.75
ppm (0.192%), 9177.36
ppm (0,918%), for qualified KB, AA, and KA respectively.
Penulis: Yulianis, Adek Zamrud
Adnan, Deddi Prima Putra
Kode Jurnal: jpfarmasidd110098
