SINTESIS SENYAWA AURIVILLIUS LAPIS EMPAT, SrBi4-xLaxTi4O15 DENGAN METODE HIDROTERMAL

Abstract: Aurivillius phases  are  metal  oxide  type  compound  with  general  formula  [Bi2O2]2+[An-1BnO3n+1]2-. Four-layers  Aurivillius  phases,  SrBi4-xLaxTi4O15  with  x  =  0.5  and  1  have  been  synthesized  by hydrothermal  method  using  NaOH  3  M  as  mineralizer  at  temperature  240oC  for  72  hours..  The products were characterized by X-ray diffraction (XRD) and SEM. All X-ray diffraction data were refined by Le Bail technique using Rietica program. The results showed that the samples formed four-layers Aurivillius phase, mixture with the perovskite phase. Increasing amount of La3+ in the sample tends to increase the perovskite phase. The morphology of the samples  was analyzed by SEM and showed plates typical compounds of Aurivillius phase.  
Keywords: Aurivillius phase, Hydrothermal Method, perovskit, Le Bail
Penulis: Zulhadjri, Hermis, dan Syukri Arief
Kode Jurnal: jpkimiadd140483

Artikel Terkait :