PENGARUH TEKNIK SINTESIS TERHADAP KUALITAS PRODUK FATTYAMINA SEKUNDER
Abstract: Secondary
fattyamines has been synthesized by reacting primary fatty amines with
acylchlorides and continued with reducing the corresponding secondary
fattyamides formed to secondary fattyamines using LiAIH<I'Fatty amines are
raw material of natural-based surfactants that can be derived from fatty acids,
olefins, or alcohols, of which can be synthesized from natural sources such as
palm oil. Conversion of secondary fatty amides to secondary fatty amines was
evaluated through the quality of FTIR spectra on wave number of 1639-1645 em'
(C=O vibration) and 1544-1555 em" (vibrations of C-H and of secondary
amine N-H). Method of synthesis by using closed reflux syncore reactor was
better than those of using microwave teflon tubes, and open reflux. The yield
of 9 different secondary fatty amines obtainedfrom 5 to 27 replicates by the
closed reflux syncore reactor method varied from 17%to 96%.
Penulis: Komar Sutriah, Zainal
Alim Mas'ud, Tun Tedja Irawadi
Kode Jurnal: jpkimiadd110179
