Abstrak: Ketalization of
glycerol and acetophenone in an azeotropic petroleum benzene solvent using
p-toluene sulfonic acid as the catalyst gave
2-methyl-2-phenyl-4-hydroxymethyl-1,3-dioksolane with 82% yiled. The product
was selectively chlorinated with phosphor trichlorida in chloroform solvent
gave 2-methyl-2-phenyl-4-kloro methyl-1,3-dioxolane with79% yield and followed
by deketalization by treatment with 1N hydrochloric acid in Tetrahydrofuran to
produce 3-chloro-1,2-propane-diol.
Keyword: Propane-diol,
glycerol, deketalization, ketalization
Penulis: Hestina, Indra Masmur
dan Daniel
Kode Jurnal: jpkimiadd100059
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